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Synthesis and crystal structure of

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dc.contributor.author Aygun, M
dc.contributor.author Cetinkaya, E
dc.contributor.author Gok, Y
dc.contributor.author Kendi, E
dc.contributor.author Cetinkaya, B
dc.date.accessioned 2022-10-19T12:19:10Z
dc.date.available 2022-10-19T12:19:10Z
dc.date.issued 2003
dc.identifier.uri http://hdl.handle.net/11616/84457
dc.description.abstract In the title compound, C23H32N4Se, was synthesized and its crystal structure was determined by single crystal X-ray diffraction. The compound crystallizes in orthorhombic system, space group Pbca, a = 10.9960(10)Angstrom, b = 14.9460(9)Angstrom, c = 27.565(5)Angstrom and Z = 2. According to X-ray crystallographic studies, the diazepine ring is observed to be in a disordered state. The site-occupancy of the major compenent refined to 0.53(1). The C=Se bond length of 1.862(4)Angstrom is a double bond character. The dihedral angle between the two phenyl rings is 37.7(2)degrees.
dc.description.abstract C1 Dokuz Eylul Univ, Dept Phys, TR-35160 Izmir, Turkey.
dc.description.abstract Inonu Univ, Dept Chem, TR-44069 Malatya, Turkey.
dc.description.abstract Hacettepe Univ, Dept Engn Phys, TR-06532 Ankara, Turkey.
dc.description.abstract Ege Univ, Dept Chem, TR-35100 Izmir, Turkey.
dc.source ANALYTICAL SCIENCES
dc.title Synthesis and crystal structure of
dc.title hexahydrobis[(1,3-p-dimethylaminobenzyl)-1,3-diazepinel-2-selenone,
dc.title C23H32N4Se


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