Aktas, Aydin2024-08-042024-08-0420190254-5861https://doi.org/10.14102/j.cnki.0254-5861.2011-2331https://hdl.handle.net/11616/99065In this paper, a new Pd-based complex that contains N-heterocyclic carbene (NHC) and triphenylphosphine (PPh3) ligands was synthesized. The cis-(NHC)PdBr2(PPh3) complex has been prepared by the substitution of 3-chloropyridine ligand in (NHC)PdBr2(3-chloropyridine) complex with triphenylphosphine. This complex has been characterized by using H-1 NMR, P-31 {H-1} NMR, C-13 {H-1} NMR, FTIR, UV-Vis spectroscopy and elemental analysis techniques. The molecular and crystal structures of the cis-(NHC)PdBr2(PPh3) complex were determined by single-crystal X-ray diffraction method.eninfo:eu-repo/semantics/closedAccessFTIRN-heterocyclic carbeneNMRUV-VISX-ray diffractionArticle38101664167210.14102/j.cnki.0254-5861.2011-23312-s2.0-85075393941Q3WOS:000502700100004Q4