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1-(Prop-2-en-1-yl)-3-[(trimethylsilyl)methyl]benzimidazolium bromide monohydrate
(Int Union Crystallography, 2010) Baktir, Zeliha; Akkurt, Mehmet; Sireci, Nihat; Kucukbay, Hasan
In the title compound, C14H21N2Si+center dot Br-center dot H2O, the benzimidazole ring system is almost planar [maximum deviation = 0.021 (2) angstrom]. In the crystal, O-H center dot center dot center dot Br and C-H center dot center dot center dot O hydrogen bonds link the ions via the O atoms of the water molecules. In addition, there are pi-pi stacking interactions between the centroids of the benzene and imidazole rings of the benzimidazole ring system [centroid-centroid distances = 3.521 (3) and 3.575 (2) angstrom].
Synthesis of 1-substituted benzimidazole metal complexes and structural characterization of dichlorobis(1-phenyl-1H-benzimidazole-?N3)cobalt(II) and dichlorobis (1-phenyl-1H-benzimidazole-?N3)zinc(II)
(Taylor & Francis Ltd, 2011) Sireci, Nihat; Yilmaz, Ulku; Kucukbay, Hasan; Akkurt, Mehmet; Baktir, Zeliha; Turktekin, Sevim; Buyukgungor, Orhan
The Co(II), Zn(II), Ni(II), Cu(II), and Fe(II) complexes of 1-phenylbenzimidazole were synthesized and characterized by NMR and elemental analyses. The crystal structures of dichlorobis(1-phenyl-1H-benzimidazole-kappa N-3) cobalt(II) and dichlorobis(1-phenyl-1H-benzimidazole-kappa N-3)zinc(II) have been determined by single-crystal X-ray diffraction.