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    Comparison of iron ores upgraded with Falcon concentrator and magnetic separators assisted by coal reduction-conversion process
    (Taylor & Francis Inc, 2020) Vapur, Huseyin; Top, Soner; Altiner, Mahmut; Uckun, Sukru; Sarikaya, Musa
    This study investigated the effects of iron ore roasting on iron ore beneficiation. Hematite-magnetite conversion was comprehensively investigated and characterized by XRD, SEM, and M-H analyses. The magnetic susceptibilities of the materials were shown by Honda-Owen plots. The optimum magnetite transformation conditions were found as 800 degrees C temperature, 10 wt.% coal and 10 min reaction time. Preliminary tests with the unroasted ores were conducted before the optimization and comparison tests. The Box Behnken test design was used for modeling the falcon concentrator separation tests. High-intensity wet magnetic, low-intensity dry magnetic and falcon gravity separators were applied to the roasted and unroasted ores at the optimum test conditions. After conversion, the iron concentrations in the grade that could be sold (>56% Fe) were obtained by the wet magnetic separator and the falcon gravity separator with the recovery yields of 90.87 and 81.72%, respectively. The positive effects of roasting were observed in terms of concentrate yields for the wet magnetic separation and gravity separation methods. However, desired saleable iron concentrates were not achieved by dry magnetic separation experiments, although the recovery yields were raised above 80% after the conversion process.
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    GAZLAŞTIRMA TESİSİ ODUN ATIĞI VE SİVAS KANGAL LİNYİT KÖMÜRÜNÜN BOYA ADSORPSİYONUNDA KULLANIM OLANAKLARININ ARAŞTIRILMASI
    (2020) Kırma, Ramazan; Sarıkaya, Musa; Top, Soner; Uçkun, Şükrü; Timür, İrfan
    Öz: Bu çalışmada Sivas Kangal linyit kömürü ile Gebze MDF ve Yonga Levha Gazlaştırma Tesisi ön çalışmalarında elde edilen odun atığının adsorban olarak kullanılma olanakları araştırılmıştır. Böylelikle hem atıkların değerlendirilmesi hem de daha ucuz ve kolay elde edilen malzemeler ile çevre kirliliğinin önlenmesi amaçlanmıştır. -75 µm boyutuna kırılıp öğütülen ve adsorban olarak kullanılan odun atığı ve kömür numunelerin yapı ve yüzey özellikleri XRD, SEM ve BET analizleri ile incelenmiştir. Ayrıca kül, nem, uçucu madde ve sabit karbon içerikleri ile elementel analizleri yapılarak numuneler karakterize edilmiştir. Deneylerde boyar madde olarak C16H18CIN3 S.xH2 O formülasyonuna sahip metilen mavisi (MM) kullanılmıştır. Sıcaklık, karıştırma süresi ve derişim parametrelerinin MM adsorpsiyonu üzerine etkileri araştırılmıştır. Optimum konsantrasyonlarda değişik sıcaklıklar için Langmuir izotermleri oluşturulmuştur. Sonuç olarak mevcut çalışma ile adsorban olarak tercihen linyit kömürü ve odun atığının kullanılabileceği ortaya konulmuştur. Linyit kömürü için 10 ppm ve odun atığı için ise 3 ppm MM konsantrasyonlarının adsorpsiyon için ideal derişimler olduğu belirlenmiştir.
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    Removal of Heavy Metals from Wastewater Solution Using a Mechanically Activated Novel Zeolitic Material
    (Pleiades Publishing Inc, 2020) Uckun, Sukru; Sarikaya, Musa; Top, Soner; Timur, Irfan
    The removal of heavy metals from the wastewater solution using a novel zeolitic material was conceived and experimentally probed. The natural zeolite was ground in a planetary ball mill to increase negative surface charge and amorphization of the material as well as a conventional ball mill. The ground materials were used for the removal of heavy metals from the wastewater solution. The maximum removals were found to be 78% for Pb, 67% for Ni and 54% for Cd by using the conventional milled natural zeolitic material at pH 11. However, 93% of Pb, 72% of Ni and 57% of Cd were removed at pH 9 with the novel zeolitic material milled by a planetary ball mill. It was revealed that the novel zeolitic material produced by a planetary ball mill increased the absorption capacity of the heavy metals and reduced the alkali requirement for pH adjustment. The removal order of heavy metals with the novel zeolitic material is determined as follows: Pb> Ni>Cd.