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    In vitro comparison of physical, chemical, and mechanical properties of graphene nanoplatelet added Angelus mineral trioxide aggregate to pure Angelus mineral trioxide aggregate and calcium hydroxide
    (Wiley, 2021) Kucukyildiz, Elif Nihan; Dayi, Burak; Altin, Serdar; Yigit, Oktay
    It is important to cover the pulp surface with a biocompatible material that is physically, mechanically, and chemically adequate. Graphene has the potential to form hard tissue, but at high doses, it shows toxic effects. It can be added to biocompatible materials at low doses to enhance their hard tissue forming potential. The aim of this study was to compare the physical, chemical, and mechanical properties of graphene nanoplatelet (GNP) added Angelus mineral trioxide aggregate (A-MTA) to pure A-MTA and calcium hydroxide. Homogeneous mixtures (created by adding +0.1 weight[wt]% and 0.3 wt% GNP to A-MTA), pure A-MTA, and Dycal were used. Three disc-shaped samples of each material were prepared using Teflon mold. Scanning electron microscope-energy dispersive X-ray (SEM-EDX), particle size, microhardness, and Fourier transform infrared spectroscopy (FTIR) analysis of the materials were performed in vitro. Data were analyzed using Kruskal-Wallis test followed by Conover test (p < .001). A-MTA and GNP added samples showed similar peaks in FTIR analysis. In the EDX analysis, the amount of carbon was observed with a higher increase at A-MTA + 0.3 wt% GNP than A-MTA + 0.1 wt% GNP. In the SEM image, hollow structure and particle size decreased as the amount of GNP increased; particle size was smaller at A-MTA + 0.3 wt% GNP than A-MTA + 0.1 wt% GNP (p < .001). A-MTA + 0.3 wt% GNP showed the highest microhardness while Dycal showed the lowest microhardness. The addition of GNP, a material with high potential for forming hard tissue, to the structure of capping materials can also positively contribute to the microhardness of the capping materials.
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    Physico-mechanical and thermal characteristics of commercially available and newly developed dental flowable composites
    (Elsevier Science Bv, 2018) Kamalak, Hakan; Canbay, C. Aksu; Yigit, Oktay; Altin, Serdar
    In this study, we investigated the structural stability, thermal conductivity, thermal analysis, materials' homogeneity of newly developed flowable composites. 6 different dental flowable composite resins; Grandio Flow (GF), Charisma Flow (CF), Tetric N Flow (TNF), Clearfil Majesty Flow (CMF),3M Filtek Ultimate Flow (3MFU), Voco Amaris Flow (VFA) were used. Restorations were made in standard teflon molds and the materials were light-cured for 20s in a 6 mm x 2 mm teflon mould. After polymerization, samples were kept in distilled water at 37 degrees C/24 h it was found that the composites have multiphase component such as metallic dopant and organic binder. The XRD investigation showed that there was a broad halo in the pattern which indicates the organic section in the composites. The FTIR results indicate the bond structure of the composites. The temperature dependence of the thermal conductivity of the composites were found below to 5 mW/K value depending on the type of the composites, which are low enough for dental application. The micro-hardness of the samples was analyzed and the result was compared. (C) 2017 Elsevier B.V. All rights reserved.