Confirmatory Method for the Determination of Volatile Congeners and Methanol in Turkish Raid According to European Union Regulation (EEC) No. 2000R2870: Single-Laboratory Validation

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dc.authoridYilmaztekin, Murat/0000-0002-5667-9169
dc.authoridCABAROGLU, TURGUT/0000-0003-1489-9929
dc.authorwosidYilmaztekin, Murat/N-9692-2013
dc.authorwosidCABAROGLU, TURGUT/G-6984-2018
dc.contributor.authorYilmaztekin, Murat
dc.contributor.authorCabaroglu, Turgut
dc.date.accessioned2024-08-04T20:57:30Z
dc.date.available2024-08-04T20:57:30Z
dc.date.issued2011
dc.departmentİnönü Üniversitesien_US
dc.description.abstractA method described by European Union Regulation (EEC) No. 2000R2870 was validated and supported by GC/MS analysis for the determination of volatile congeners and methanol in Turkish raki. The method was validated in terms of specificity, accuracy, precision, LOD, LOQ, linearity, and robustness. The specificity of the method was demonstrated, and the method showed excellent accuracy (97.5-100.1%). Linearity was checked in the ranges of 0.200-26.390 mg/100 mL for more volatile compounds and 1.155-48.00 mg/100 mL for less volatile compounds, after concentrations found in Turkish raki were taken into account. The calibration curves of all analytes showed good linearity (R-2 > 0.998). The within- and between-day precision (RSD) values of 11 analytes were in the range. of 0.18-4.50%. The LOD and LOQ values were in the range of 0.014-0.362 and 0.045-1.085 mg/100 mL, respectively. The method can be used as an absolute quantification method for the determination of volatile congeners and methanol in Turk ish raki and for QC.en_US
dc.identifier.endpage617en_US
dc.identifier.issn1060-3271
dc.identifier.issn1944-7922
dc.identifier.issue2en_US
dc.identifier.pmid21563697en_US
dc.identifier.startpage611en_US
dc.identifier.urihttps://hdl.handle.net/11616/102691
dc.identifier.volume94en_US
dc.identifier.wosWOS:000289544500030en_US
dc.identifier.wosqualityQ2en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakPubMeden_US
dc.language.isoenen_US
dc.publisherAoac Inten_US
dc.relation.ispartofJournal of Aoac Internationalen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectLiquid-Chromatographyen_US
dc.titleConfirmatory Method for the Determination of Volatile Congeners and Methanol in Turkish Raid According to European Union Regulation (EEC) No. 2000R2870: Single-Laboratory Validationen_US
dc.typeArticleen_US

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