Sol-gel synthesis of 3-(triethoxysilyl)propylsuccinicanhydride containing fluorinated silane for hydrophobic surface applications

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dc.authoridKiraz, Nadir/0000-0002-6858-2946
dc.authoridkesmez, ömer/0000-0003-0107-8558
dc.authoridCamurlu, Hasan Erdem/0000-0003-3170-4492
dc.authoridAkarsu, Esin/0000-0002-1965-5774
dc.authorwosidAsilturk, Meltem/B-2989-2013
dc.authorwosidArpac, Ertugrul/C-5471-2016
dc.authorwosidKiraz, Nadir/C-1687-2016
dc.authorwosidkesmez, ömer/I-7153-2017
dc.authorwosidCamurlu, Hasan Erdem/C-2534-2016
dc.authorwosidAkarsu, Esin/C-5410-2016
dc.contributor.authorKiraz, Nadir
dc.contributor.authorBurunkaya, Esin
dc.contributor.authorKesmez, Omer
dc.contributor.authorAsilturk, Meltem
dc.contributor.authorCamurlu, H. Erdem
dc.contributor.authorArpac, Ertugrul
dc.date.accessioned2024-08-04T21:01:10Z
dc.date.available2024-08-04T21:01:10Z
dc.date.issued2010
dc.departmentİnönü Üniversitesien_US
dc.description.abstractIn this paper, novel fluorinated silane compound was prepared by adding hydroxyl terminated Fluorolink D10H oligomer to 3-(triethoxysilyl)propylsuccinicanhydride. The obtained silane system was independently composed with 3-Aminopropyltrimethoxysilane, 3-Glycidyloxypropyltrimethoxysilane and 3-Glycidyloxypropyltriethoxysilane and, then the prepared coating solutions were applied to glass surface by spin-coating method. The chemical bonding between groups in system was investigated by Fourier Transform Infrared Spectroscopy analyses. The elemental composition of coatings was determined using Energy Dispersive X-ray Spectroscopy analyses. Its structure and surface properties were analyzed by scanning electron microscopy, atomic force microscopy, contact angle measurement and Ultraviolet-visible Absorption Spectroscopy. The amounts of fluorine on the coatings prepared with GF20-D10H-AMMO, GF20-D10H-GLYEO and GF20-D10H-GLYMO are 31, 32 and 34% at, respectively. Transparent coatings with smooth surface and uniform thickness were observed. The coatings had nanoscale roughness. The contact angles of coatings for water ranged from 88 to 107(o), and that of n-hexadecane ranged from 53 to 60(o).en_US
dc.description.sponsorshipAkdeniz University; NANOen Ar-Ge Ltd.Sti.en_US
dc.description.sponsorshipAuthors would like to thank Akdeniz University Research Fund for financial support. Technical and financial support of NANOen Ar-Ge Ltd.Sti. is gratefully acknowledged.en_US
dc.identifier.doi10.1007/s10971-010-2289-3
dc.identifier.endpage166en_US
dc.identifier.issn0928-0707
dc.identifier.issue2en_US
dc.identifier.startpage157en_US
dc.identifier.urihttps://doi.org/10.1007/s10971-010-2289-3
dc.identifier.urihttps://hdl.handle.net/11616/104153
dc.identifier.volume56en_US
dc.identifier.wosWOS:000283370400009en_US
dc.identifier.wosqualityQ1en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.language.isoenen_US
dc.publisherSpringeren_US
dc.relation.ispartofJournal of Sol-Gel Science and Technologyen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectFluorinated silaneen_US
dc.subjectSol-gelen_US
dc.subjectHydrophobicityen_US
dc.subjectOleophobicityen_US
dc.subjectTransparent coatingsen_US
dc.titleSol-gel synthesis of 3-(triethoxysilyl)propylsuccinicanhydride containing fluorinated silane for hydrophobic surface applicationsen_US
dc.typeArticleen_US

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