Hydrothermal synthesis and characterization of nanocrystalline ZrO2 and surface modification with 2-acetoacetoxyethyl methacrylate

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dc.authoridOKUSLUK, Funda/0000-0002-1334-4043
dc.authoridAkarsu, Esin/0000-0002-1965-5774
dc.authorwosidOKUSLUK, Funda/ABG-8842-2020
dc.authorwosidAsilturk, Meltem/B-2989-2013
dc.authorwosidArpac, Ertugrul/C-5471-2016
dc.authorwosidAkarsu, Esin/C-5410-2016
dc.contributor.authorSayilkan, Funda
dc.contributor.authorAsilturk, Meltem
dc.contributor.authorBurunkaya, Esin
dc.contributor.authorArpac, Ertugrul
dc.date.accessioned2024-08-04T20:31:15Z
dc.date.available2024-08-04T20:31:15Z
dc.date.issued2009
dc.departmentİnönü Üniversitesien_US
dc.description.abstractFor the utilization as inorganic/organic hybrid nanomaterials for optical purposes, nanocrytalline tetragonal ZrO2 was synthesized by hydrothermal method using zirconium(IV)-n-propoxide as precursor material. Surface of the ZrO2 particles was then modified with 2-acetoacetoxyethyl methacrylate used as a copolymer for coatings. X-ray diffraction analysis revealed that both ZrO2 and modified ZrO2 are in tetragonal crystalline phase. As proved by transmission electron microscope and particle size analysis, average particle sizes of ZrO2 and modified ZrO2 were found as 6.22 and 14.7 nm, respectively. ZrO2 powder was easily dispersed either in water or n-hexane. Ultraviolet diffuse reflectance spectrophotometer analysis for ZrO2 and surface modified ZrO2 showed that maximum absorption peaks are at 215 and 225 nm, respectively.en_US
dc.description.sponsorshipScientific and Technological Research Council of Turkey (TUBITAK) [107M253]en_US
dc.description.sponsorshipThis work is dedicated to the memory of our team leader Prof. Dr. Hikmet Sayilkan (1962-2008). The authors wish to thank Dr. Murat Erdemoglu for his limitless contribution during preparation and revising the manuscript, and Can Simsek for his precious assistance in the laboratory. The authors gratefully acknowledge financial support of the Scientific and Technological Research Council of Turkey (TUBITAK) with Grant No. 107M253.en_US
dc.identifier.doi10.1007/s10971-009-1970-x
dc.identifier.endpage189en_US
dc.identifier.issn0928-0707
dc.identifier.issn1573-4846
dc.identifier.issue2en_US
dc.identifier.scopus2-s2.0-67650221349en_US
dc.identifier.scopusqualityQ2en_US
dc.identifier.startpage182en_US
dc.identifier.urihttps://doi.org/10.1007/s10971-009-1970-x
dc.identifier.urihttps://hdl.handle.net/11616/94831
dc.identifier.volume51en_US
dc.identifier.wosWOS:000267367300008en_US
dc.identifier.wosqualityQ1en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherSpringeren_US
dc.relation.ispartofJournal of Sol-Gel Science and Technologyen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectTransmission electron microscopy (TEM)en_US
dc.subjectX-ray diffraction (XRD)en_US
dc.subjectNanocrystalline materialsen_US
dc.subjectNanostructureen_US
dc.subjectZrO2en_US
dc.subjectHydrothermal synthesisen_US
dc.titleHydrothermal synthesis and characterization of nanocrystalline ZrO2 and surface modification with 2-acetoacetoxyethyl methacrylateen_US
dc.typeArticleen_US

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