Crystal structure of (2E)-3-(2-thienyl)acrylic acid-benzene-1,2-diamine

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dc.authorscopusid14832237900
dc.authorscopusid35793361300
dc.authorscopusid24173773700
dc.authorscopusid6701563510
dc.authorscopusid36039473500
dc.contributor.authorAkkurt M.
dc.contributor.authorYildirim S.O.
dc.contributor.authorŞreci N.
dc.contributor.authorKüçükbay H.
dc.contributor.authorBüyükgüngör O.
dc.date.accessioned2024-08-04T20:02:20Z
dc.date.available2024-08-04T20:02:20Z
dc.date.issued2007
dc.departmentİnönü Üniversitesien_US
dc.description.abstractThe title compound, (2E)-3-(2-thienyl)acrylic acid-benzene-1,2-diamine, was synthesized by the reaction of 1,2-diaminobenzen and 3-(2-tienyl)acrylic acide in a dioxane solution. The compound crystallizes in the orthorhombic space group Pbcn; a = 24.610(5)Å, b = 7.588(5)Å, c = 11.289(5)Å, V = 2108.1(17)Å3 and Z = 8. The final R value is 0.047. The thiophene and benzene ring are each essentially planar. The benzene-1,2-diamine moity in the title compound has a rotation axis that passes through the mid point of the bonds C8-C8a and C10-C10a. The crystal packing is stabilized by intermolecular N-H···and O-H···N hydrogen-bonding interactions. 2007 © The Japan Society for Analytical Chemistry.en_US
dc.identifier.doi10.2116/analscix.23.x233
dc.identifier.endpagex234en_US
dc.identifier.issn1348-2238
dc.identifier.issue11en_US
dc.identifier.scopus2-s2.0-70649105631en_US
dc.identifier.scopusqualityN/Aen_US
dc.identifier.startpagex233en_US
dc.identifier.urihttps://doi.org/10.2116/analscix.23.x233
dc.identifier.urihttps://hdl.handle.net/11616/91618
dc.identifier.volume23en_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherJapan Society for Analytical Chemistryen_US
dc.relation.ispartofAnalytical Sciences: X-ray Structure Analysis Onlineen_US
dc.relation.publicationcategoryDiğeren_US
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.subject[No Keyword]en_US
dc.titleCrystal structure of (2E)-3-(2-thienyl)acrylic acid-benzene-1,2-diamineen_US
dc.typeNoteen_US

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