The effects of Ni-addition on the crystal structure, thermal properties and morphology of Mg-based hydroxyapatites synthesized by a wet chemical method
Küçük Resim Yok
Tarih
2018
Dergi Başlığı
Dergi ISSN
Cilt Başlığı
Yayıncı
Elsevier Sci Ltd
Erişim Hakkı
info:eu-repo/semantics/closedAccess
Özet
Four Mg-based hydroxyapatites (HAps) doped with Ni at various amounts of 0, 0.6, 1.2 and 1.8 at% were prepared at the temperature of 870 degrees C by a wet chemical synthesis. The crystallite size, lattice parameters and crystallinity percent dramatically decreased with adding of Ni. The amount of HAp phase for all the Ni-containing samples is smaller than that of the Ni-free MgHAp. Furthermore, the lattice strain, stress and anisotropic energy density values were affected by the amount of Ni. The differential thermal analysis (DTA) measurements taken in the temperature range from 25 to 1000 degrees C showed that all the samples are thermally stable. No significant change in the morphology was observed. It was observed that the gradual introduction of Ni caused the Ca-deficiency.
Açıklama
Anahtar Kelimeler
Hydroxyapatite, Wet chemical method, X-ray diffraction (XRD), Morphology
Kaynak
Ceramics International
WoS Q Değeri
Q1
Scopus Q Değeri
Q1
Cilt
44
Sayı
12
