Preparation of aluminum-doped zinc oxide (AZO) nano particles by hydrothermal synthesis

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dc.authoridkesmez, ömer/0000-0003-0107-8558
dc.authoridKiraz, Nadir/0000-0002-6858-2946
dc.authoridAkarsu, Esin/0000-0002-1965-5774
dc.authoridCamurlu, Hasan Erdem/0000-0003-3170-4492
dc.authorwosidkesmez, ömer/I-7153-2017
dc.authorwosidKiraz, Nadir/C-1687-2016
dc.authorwosidArpac, Ertugrul/C-5471-2016
dc.authorwosidAsilturk, Meltem/B-2989-2013
dc.authorwosidAkarsu, Esin/C-5410-2016
dc.authorwosidCamurlu, Hasan Erdem/C-2534-2016
dc.contributor.authorBurunkaya, Esin
dc.contributor.authorKiraz, Nadir
dc.contributor.authorKesmez, Oemer
dc.contributor.authorCamurlu, H. Erdem
dc.contributor.authorAsilturk, Meltem
dc.contributor.authorArpac, Ertugrul
dc.date.accessioned2024-08-04T20:35:41Z
dc.date.available2024-08-04T20:35:41Z
dc.date.issued2010
dc.departmentİnönü Üniversitesien_US
dc.description.abstractAluminum doped zinc oxide (AZO) nanometric particles were synthesized by hydrothermal method. Aluminum nitrate hydrate, aluminum sec-butoxide and zinc nitrate hydrate were used as the starting materials, and n-propanol and 2-butanol were used as solvents. Ratio of Al2O3 in ZnO was kept at 10 wt%. Reaction was conducted in a Teflon autoclave at 175-225 A degrees C for 5 h. Ratios of alcohol, H2O and HCl to zinc nitrate hydrate were altered and 6 different sets of parameters were investigated. Obtained products were subjected to powder-XRD, particle size measurement, TEM examination and AAS analysis. Single phase AZO particles were obtained at alcohol to zinc nitrate ratio of 35, acid to zinc nitrate ratio of 0.2, at 225 A degrees C. Particle size was determined as 3.2 +/- A 0.4 nm from TEM examinations and as 1-2 nm from dynamic light scattering. Synthesized particles have amphiphilic character, thus they can be dispersed in both polar and non-polar media. It was seen from the UV-diffuse reflectance spectra that the AZO powder had low reflectance in the UV region and high reflectance in the visible region. The obtained powder has the potential to be utilized in the form of thin films for optical and electronic purposes.en_US
dc.description.sponsorshipScientific and Technological Research Council of Turkey (TUBITAK) [107M253]; Akdeniz University; NANOen; Matteken_US
dc.description.sponsorshipThe authors gratefully acknowledge financial support of the Scientific and Technological Research Council of Turkey (TUBITAK) with Grant No. 107M253. Authors thank Akdeniz University Research Fund for financial support. Technical and financial support of NANOen and Mattek is gratefully acknowledged.en_US
dc.identifier.doi10.1007/s10971-010-2229-2
dc.identifier.endpage176en_US
dc.identifier.issn0928-0707
dc.identifier.issn1573-4846
dc.identifier.issue2en_US
dc.identifier.scopus2-s2.0-84455191460en_US
dc.identifier.scopusqualityQ2en_US
dc.identifier.startpage171en_US
dc.identifier.urihttps://doi.org/10.1007/s10971-010-2229-2
dc.identifier.urihttps://hdl.handle.net/11616/95520
dc.identifier.volume55en_US
dc.identifier.wosWOS:000280249700005en_US
dc.identifier.wosqualityQ1en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherSpringeren_US
dc.relation.ispartofJournal of Sol-Gel Science and Technologyen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectSol-gel processesen_US
dc.subjectHydrothermal synthesisen_US
dc.subjectAluminum doped zinc oxide (AZO)en_US
dc.subjectNanoparticleen_US
dc.titlePreparation of aluminum-doped zinc oxide (AZO) nano particles by hydrothermal synthesisen_US
dc.typeArticleen_US

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