Determination of antimony by using tungsten trap atomic absorption spectrometry

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dc.authoridBAKIRDERE, Sezgin/0000-0001-9746-3682;
dc.authorwosidBAKIRDERE, Sezgin/ABU-6359-2022
dc.authorwosidArslan, Yasin/KJL-4344-2024
dc.authorwosidDURAN, SERAP TİTRETİR/AAF-7927-2020
dc.authorwosidkendüzler, erdal/AAG-4586-2019
dc.contributor.authorTitretir, Serap
dc.contributor.authorKenduezler, Erdal
dc.contributor.authorArslan, Yasin
dc.contributor.authorKula, Ibrahim
dc.contributor.authorBakirdere, Sezgin
dc.contributor.authorAtaman, O. Yavuz
dc.date.accessioned2024-08-04T20:30:56Z
dc.date.available2024-08-04T20:30:56Z
dc.date.issued2008
dc.departmentİnönü Üniversitesien_US
dc.description35th Biennial Colloquium Spectroscopicum Internationale -- SEP 23-27, 2007 -- Xiamen, PEOPLES R CHINAen_US
dc.description.abstractAn electrically heated tungsten coil was used as a trap in the determination of antimony. The technique consists of three steps. Initially, SbH(3) is formed by hydride generation procedure; then the analyte species in vapor form are transported to W-coil trap heated at 370 degrees C. Following the preconcentration step, the trap is heated to 895 degrees C; analyte species are revolatilized and transported to the flame-heated quartz atom cell where atornization and the formation of signal take place. The experimental parameters were optimized both for trap and no-trap studies. The most important experimental parameters are concentrations of HCI and NaBH4 solutions. H2 and At gas flow rates. and collection and revolatilization temperatures of W-coil. Accuracy was tested using a certified reference material, waste water EU-L-1. Limit of detection for the system is 16 ng 1- 1 using a sample of 36 ml collected in 4.0 min. Enhancement factor in sensitivity was 17. (c) 2008 Elsevier B.V. All rights reserved.en_US
dc.description.sponsorshipChinese Chem Soc,Chinese Phys Soc,Chinese Spectroscopy Soc,Natl Nat Sci Fdn China,Xiamen Municipal Govt,Xiamen Univen_US
dc.identifier.doi10.1016/j.sab.2008.03.021
dc.identifier.endpage879en_US
dc.identifier.issn0584-8547
dc.identifier.issue8en_US
dc.identifier.scopus2-s2.0-47649117278en_US
dc.identifier.scopusqualityQ2en_US
dc.identifier.startpage875en_US
dc.identifier.urihttps://doi.org/10.1016/j.sab.2008.03.021
dc.identifier.urihttps://hdl.handle.net/11616/94596
dc.identifier.volume63en_US
dc.identifier.wosWOS:000258815800009en_US
dc.identifier.wosqualityQ1en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherPergamon-Elsevier Science Ltden_US
dc.relation.ispartofSpectrochimica Acta Part B-Atomic Spectroscopyen_US
dc.relation.publicationcategoryKonferans Öğesi - Uluslararası - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectantimonyen_US
dc.subjecthydride generationen_US
dc.subjectW-trapen_US
dc.subjectatomic absorption spectrometryen_US
dc.subjectin-situ preconcentrationen_US
dc.titleDetermination of antimony by using tungsten trap atomic absorption spectrometryen_US
dc.typeConference Objecten_US

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